1U7U
Phosphopantothenoylcysteine synthetase from E. coli
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-08-08 |
Detector | MARRESEARCH |
Wavelength(s) | 0.95 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 52.930, 57.255, 78.756 |
Unit cell angles | 90.00, 108.86, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.400 |
R-factor | 0.236 |
Rwork | 0.221 |
R-free | 0.27900 |
Structure solution method | MAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.730 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.400 |
Rmerge | 0.054 |
Number of reflections | 8804 |
Completeness [%] | 99.9 |
Redundancy | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | PEG 3350, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 293K |