1U5W
Crystal structure of hypothetical protein yjjX from Escherichia coli
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2003-01-21 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.980312 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 70.996, 129.336, 85.378 |
| Unit cell angles | 90.00, 90.23, 90.00 |
Refinement procedure
| Resolution | 50.000 - 2.300 |
| R-factor | 0.278 |
| Rwork | 0.200 |
| R-free | 0.25500 |
| Structure solution method | SAD |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.075 | 0.075 |
| Number of reflections | 62056 | |
| <I/σ(I)> | 10.55 | 10.5 |
| Completeness [%] | 89.5 | 91.4 |
| Redundancy | 2.6 | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 298 | Li sulfate, MPD, Tris, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
