1U0U
An Aldol Switch Discovered in Stilbene Synthases Mediates Cyclization Specificity of Type III Polyketide Synthases: Pine stilbene synthase structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2000-04-24 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.933 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 57.221, 361.291, 57.317 |
Unit cell angles | 90.00, 98.39, 90.00 |
Refinement procedure
Resolution | 54.100 - 2.110 |
R-factor | 0.225 |
Rwork | 0.225 |
R-free | 0.28900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bi5 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.400 |
Data scaling software | PROW |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.100 | 2.230 |
High resolution limit [Å] | 2.110 | 2.100 |
Number of reflections | 103258 | |
Completeness [%] | 78.7 | 38.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | PEG 8000, ammonium acetate, MOPSO-Na+, DTT, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |