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1TOM

ALPHA-THROMBIN COMPLEXED WITH HIRUGEN

Experimental procedure
Spacegroup nameC 1 2 1
Unit cell lengths71.250, 72.190, 73.110
Unit cell angles90.00, 101.85, 90.00
Refinement procedure
Resolution6.000

*

- 1.800
R-factor0.172
Rwork0.172
RMSD bond length0.014
RMSD bond angle2.900
Phasing softwareX-PLOR
Refinement softwareX-PLOR
Data quality characteristics
 Overall
High resolution limit [Å]1.800

*

Rmerge0.079

*

Total number of observations40601

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Number of reflections23015

*

Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

*

7.3

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropthrombin-hirugen complex3.7 (mg/ml)
21dropsodium phosphate0.05 (M)
31drop0.375 (M)
41drop0.5 (mM)
51reservoirphosphate0.1 (M)
61reservoir1 (mM)
71reservoirPEG800030 (%(w/v))

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PDB entries from 2024-09-18

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