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1TF6

CO-CRYSTAL STRUCTURE OF XENOPUS TFIIIA ZINC FINGER DOMAIN BOUND TO THE 5S RIBOSOMAL RNA GENE INTERNAL CONTROL REGION

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X12B
Synchrotron siteNSLS
BeamlineX12B
Temperature [K]113
Detector technologyIMAGE PLATE
Collection date1996-10
DetectorMARRESEARCH
Spacegroup nameP 1
格子定数 [Å]64.180, 64.712, 78.035
格子定数 [度]90.07, 92.98, 102.95
精密化法
残基8.000 - 3.100
R因子0.308
Rwork0.308
R-free0.36300
Structure solution methodMIR
結合長の平均二乗偏差(RMSD) [Å]0.005
結合角の平均二乗偏差(RMSD) [度]0.900
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCCP4
Refinement softwareX-PLOR (3.851)
Quality characteristics
 Overall
分解能 [Å] (低)25.000
分解能 [Å] (高)3.000
Rmerge_l_obs0.128
Total number of observations126746

*

独立反射数19034
完全性 [%]77.4
冗長性6.7
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, HANGING DROP8291COMPLEX WAS CRYSTALLIZED FROM 22.5% PEG 4000, 165 MM NACL, 35 MM SODIUM ACETATE, 3.2 MM DTT, 9.2% (VOL/VOL) GLYCEROL, 1.8 MM NAN3, 1.8 MM CADAVERINE-2HCL, 5.5 MM TRIS-HCL, PH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 291.00K
結晶化試薬
ID結晶ID濃度試薬名濃度 (単位)詳細
111WATER
1012WATER
1112PEG 4000
211NACL
311SODIUM ACETATE
411DTT
511GLYCEROL
611NAN3
711CADAVERINE-2HCL
811TRIS-HCL
911PEG 4000

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件を2024-09-18に公開中

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