1T04
Three dimensional structure of a humanized anti-IFN-Gamma Fab in C2 space group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-04-20 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 82.274, 169.805, 72.825 |
Unit cell angles | 90.00, 97.68, 90.00 |
Refinement procedure
Resolution | 25.000 - 3.000 |
R-factor | 0.217 |
Rwork | 0.217 |
R-free | 0.29300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1t3f |
RMSD bond length | 0.007 |
RMSD bond angle | 1.390 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.146 | 0.387 |
Number of reflections | 19324 | |
<I/σ(I)> | 6.14 | 2.27 |
Completeness [%] | 97.1 | 96.9 |
Redundancy | 2.49 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 288 | PEG8000, (NH4)2SO4, MgCl2, MES, pH 5.60, VAPOR DIFFUSION, SITTING DROP, temperature 288K |