1STH
TWO DISTINCTLY DIFFERENT METAL BINDING MODES ARE SEEN IN X-RAY CRYSTAL STRUCTURES OF STAPHYLOCOCCAL NUCLEASE-COBALT(II)-NUCLEOTIDE COMPLEXES
Experimental procedure
Spacegroup name | P 41 |
Unit cell lengths | 47.480, 47.480, 63.210 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.850 |
R-factor | 0.174 |
Rwork | 0.174 |
RMSD bond length | 0.014 |
RMSD bond angle | 25.100 * |
Phasing software | X-PLOR (3.0) |
Refinement software | X-PLOR (3.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 6.000 * |
High resolution limit [Å] | 1.850 * |
Rmerge | 0.048 * |
Total number of observations | 87667 * |
Number of reflections | 11570 * |
Completeness [%] | 99.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 20 (mg/ml) | |
2 | 1 | drop | potassium phosphate | 10.5 (mM) | |
3 | 1 | drop | MPD | 17 (%) | |
4 | 1 | drop | pdTp | 2 (mg/ml) | |
5 | 1 | drop | 10 (mM) | ||
6 | 1 | drop | potassium citrate | 20 (mM) | |
7 | 1 | reservoir | MPD | 21-23 (%(w/w)) | |
8 | 1 | reservoir | potassium phosphate | 10.5 (mM) |