1SR9
Crystal Structure of LeuA from Mycobacterium tuberculosis
Experimental procedure
Experimental method | MAD |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Collection date | 2003-07-08 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.250, 154.730, 68.820 |
Unit cell angles | 90.00, 98.05, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.000 |
R-factor | 0.17 |
Rwork | 0.169 |
R-free | 0.19700 |
Structure solution method | MAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.470 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 74305 | |
Completeness [%] | 98.4 | 94.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.25 | 291 | sodium citrate, MPEG2000, pH 6.25, VAPOR DIFFUSION, SITTING DROP, temperature 291K |