1RNM
RIBONUCLEASE A COMPLEX WITH CYTIDYLIC ACID (5'CMP) CRYSTALLIZED FROM 80% AMMONIUM SULPHATE
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 290 |
Detector technology | AREA DETECTOR |
Collection date | 1992 |
Detector | SIEMENS |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 65.630, 65.630, 65.380 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.000 |
R-factor | 0.158 |
Rwork | 0.158 |
RMSD bond length | 0.012 |
RMSD bond angle | 2.470 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | X-PLOR |
Refinement software | PROFFT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 9.600 | 2.090 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.044 | 0.127 |
Number of reflections | 8914 | |
<I/σ(I)> | 41.2 | 9.6 |
Completeness [%] | 78.3 | 51.2 |
Redundancy | 2.58 | 1.68 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | pH 5.5 |