1RLD
SOLID-STATE PHASE TRANSITION IN THE CRYSTAL STRUCTURE OF RIBULOSE 1,5-BIPHOSPHATE CARBOXYLASE(SLASH)OXYGENASE
Experimental procedure
Spacegroup name | I 4 |
Unit cell lengths | 153.010, 153.010, 113.450 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.500 |
R-factor | 0.211 |
Rwork | 0.211 |
RMSD bond length | 0.018 |
RMSD bond angle | 3.830 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.500 * |
Rmerge | 0.083 * |
Number of reflections | 38575 * |
Completeness [%] | 84.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5.2 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | 0.2 (M) | ||
2 | 1 | reservoir | 0.3 (M) | ||
3 | 1 | reservoir | 1 (mM) | ||
4 | 1 | drop | precipitant | 30-70 (%(v/v)) |