1RKE

Human vinculin head (1-258) in complex with human vinculin tail (879-1066)

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2.35 Å)

Cell axes86.603161.64836.040
Cell angles90.0090.0090.00
SpacegroupP 21 21 2
Resolution limits15.00 - 2.35
the highest resolution shell value2.420 - 2.350
R-work0.20600
the highest resolution shell value0.205
R-free0.27800
the highest resolution shell value0.277
RMSD bond length0.008
RMSD bond angle0.979

Data Collection Statistics

Resolution limits99.80 - 2.35
the highest resolution shell value -
Number of reflections21798
I/sigma(I)0

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1Vapor diffusion*8293R.T.*

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirPEG335015 (%)
21reservoir50 (mM)
31reservoirTris100 (mM)pH8
41reservoirdithiothreitol10 (mM)
Annotated Information is extracted from Literature Info*
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