1RFX
Crystal Structure of resisitin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X4A |
| Synchrotron site | NSLS |
| Beamline | X4A |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Collection date | 2002-06-14 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.54975 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 44.298, 174.670, 90.163 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 14.860 - 2.002 |
| R-factor | 0.17915 |
| Rwork | 0.177 |
| R-free | 0.21597 |
| Structure solution method | SAD |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.230 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SHARP |
| Refinement software | REFMAC (5.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.070 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.071 | 0.213 |
| Number of reflections | 24119 | |
| <I/σ(I)> | 25 | 9.6 |
| Completeness [%] | 97.4 | 95.2 |
| Redundancy | 25.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 2 | 277 | 0.1M Sodium acetate, 8% PEG 4000, 0.1M Potassium Chloride, pH 2., VAPOR DIFFUSION, HANGING DROP, temperature 277K |
