1RBJ

RIBONUCLEASE B COMPLEX WITH D(TETRA-(DEOXY-ADENYLATE))

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Detector technology	DIFFRACTOMETER
Collection date	1984-09-11
Detector	ENRAF-NONIUS CAD4
Spacegroup name	P 41 21 2
Unit cell lengths	44.450, 44.450, 156.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.700
R-factor	0.163
RMSD bond length	0.020
RMSD bond angle	2.982
Data reduction software	ORESTES
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.600
Rmerge	0.040
Number of reflections	3431
Completeness [%]	69.5
Redundancy	2. *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		277	VAPOR DIFFUSION, temperature 277.00K