1R8I
Crystal structure of TraC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-BM |
Synchrotron site | APS |
Beamline | 19-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-08-24 |
Detector | CUSTOM-MADE |
Wavelength(s) | 0.97931 |
Spacegroup name | H 3 2 |
Unit cell lengths | 144.015, 144.015, 91.880 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.000 * - 3.000 |
R-factor | 0.263 |
Rwork | 0.263 |
R-free | 0.28830 * |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.380 * |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.068 * | 0.301 * |
Total number of observations | 106523 * | |
Number of reflections | 13072 | |
<I/σ(I)> | 21.4 | 3.2 |
Completeness [%] | 92.1 | 92.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.25 | 293 | ammonium sulfate, sodium citrate, sodium chloride, glycerol, pH 6.25, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 1.26-1.34 (M) | |
2 | 1 | reservoir | sodium cirtate | 100 (mM) | pH6.25 |
3 | 1 | reservoir | 0.2 (M) | ||
4 | 1 | reservoir | glycerol | 5 (%) |