1QVY
Crystal structure of RhoGDI K(199,200)R double mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 120 |
Detector technology | CCD |
Collection date | 2002-07-03 |
Detector | CUSTOM-MADE |
Wavelength(s) | 0.9190 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 148.660, 58.240, 75.050 |
Unit cell angles | 90.00, 92.49, 90.00 |
Refinement procedure
Resolution | 27.020 - 1.600 |
R-factor | 0.17281 |
Rwork | 0.172 |
R-free | 0.20998 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1kmt |
RMSD bond length | 0.016 |
RMSD bond angle | 1.719 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.053 | 0.382 |
Number of reflections | 84662 | |
<I/σ(I)> | 15.2 | 2.7 |
Completeness [%] | 99.6 | 99.4 |
Redundancy | 3.7 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 294 | 30% PEG 400, 0.1 M Tris, 0.2 M lithium sulfate, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 294.0K |