1QGD
TRANSKETOLASE FROM ESCHERICHIA COLI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1994-07 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.850, 126.000, 151.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.900 |
Rwork | 0.132 |
R-free | 0.17600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1trk |
RMSD bond length | 0.014 |
RMSD bond angle | 0.030 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.100 | 0.323 |
Number of reflections | 503703 | |
<I/σ(I)> | 16.3 | 4.3 |
Completeness [%] | 98.2 | 97.1 |
Redundancy | 4.68 | 3.29 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.4 | pH 6.4 |