1PZA

THE CRYSTAL STRUCTURES OF REDUCED PSEUDOAZURIN FROM ALCALIGENES FAECALIS S-6 AT TWO PH VALUES

Experimental procedure

Spacegroup name	P 65
Unit cell lengths	49.900, 49.900, 99.100
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.178
RMSD bond length	0.178 *
RMSD bond angle	0.017 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.050 *
Total number of observations	67800 *
Number of reflections	12660 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	8 *		Petratos, K., (1987) FEBS Lett., 218, 209. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	1.5 (%)
2	1	drop	potassium phosphate	50 (mM)
3	1	drop	ammonium sulfate	1.5 (M)
4	1	reservoir	ammonium sulfate	3.0 (M)