1PVX
DO-1,4-BETA-XYLANASE, ROOM TEMPERATURE, PH 4.5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1997-02-03 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.762, 54.058, 90.064 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.590 |
R-factor | 0.191 |
Rwork | 0.191 |
R-free | 0.21900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yna |
RMSD bond length | 0.015 |
RMSD bond angle | 1.300 |
Data reduction software | AUTOMAR |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.700 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmerge | 0.093 | 0.358 |
Number of reflections | 24200 | |
<I/σ(I)> | 25.71 | 3.19 |
Completeness [%] | 92.5 | 78 |
Redundancy | 5.13 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | pH 4.50 |