1POP
X-RAY CRYSTALLOGRAPHIC STRUCTURE OF A PAPAIN-LEUPEPTIN COMPLEX
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.920, 104.960, 50.970 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 * - 2.100 |
R-factor | 0.198 * |
RMSD bond length | 0.013 |
RMSD bond angle | 2.330 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.100 * |
Rmerge | 0.094 * |
Number of reflections | 12452 * |
Completeness [%] | 88.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | H2O-methanol | 0.5ml | |
2 | 1 | reservoir | 0.060mlsat | ||
3 | 1 | drop | inhibited papain | 0.030ml |