1PO2
POLIOVIRUS (TYPE 1, MAHONEY) IN COMPLEX WITH R77975, AN INHIBITOR OF VIRAL REPLICATION
Experimental procedure
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-13 |
Temperature [K] | 261 |
Collection date | 1995 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 322.940, 358.040, 380.150 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 2.900 |
R-factor | 0.249 * |
Rwork | 0.249 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | REFINED STRUCTURE OF P1/MAHONEY (2PLV) AFTER OMITTING ALL LIGANDS SOLVENT AND ANY AMINO ACID LOCATED CLOSE TO A SIGNIFICANT ELECTRON DENSITY FEATURE IN THE NON-CRYSTALLOGRAPHIC SYMMETRY-AVERAGED DIFFERENCE MAP. |
RMSD bond length | 0.012 |
RMSD bond angle | 26.000 * |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.900 |
Rmerge | 0.148 |
Total number of observations | 587697 * |
Number of reflections | 306408 |
Completeness [%] | 24.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * | 7 | pH 7. |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ethylene glycol | 25 (%(v/v)) | |
2 | 1 | 1 | NaPIPES | 10 (mM) | |
3 | 1 | 1 | 5 (mM) | ||
4 | 1 | 1 | 1 (mM) |