1PNT
CRYSTAL STRUCTURE OF BOVINE HEART PHOSPHOTYROSYL PHOSPHATASE AT 2.2 ANGSTROMS RESOLUTION
Experimental procedure
Spacegroup name | C 1 2 1 |
Unit cell lengths | 95.300, 43.300, 41.200 |
Unit cell angles | 90.00, 113.50, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.200 |
R-factor | 0.166 |
Rwork | 0.166 |
RMSD bond length | 0.010 |
RMSD bond angle | 2.090 |
Phasing software | X-PLOR |
Refinement software | TNT |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.200 * |
Rmerge | 0.060 * |
Completeness [%] | 90.0 * |
Redundancy | 3.1 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.5 * | Zhang, M., (1994) J.Mol.Biol., 238, 281. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG3350 | 20 (%) | |
2 | 1 | reservoir | Tris-HCl | 50 (mM) | |
3 | 1 | reservoir | 50 (mM) |