1PNL

PENICILLIN ACYLASE HAS A SINGLE-AMINO-ACID CATALYTIC CENTRE

Experimental procedure

Spacegroup name	P 1
Unit cell lengths	52.120, 65.080, 76.300
Unit cell angles	100.20, 111.44, 105.81

Refinement procedure

Resolution	6.000 - 2.500
R-factor	0.1524
R-free	0.21500
RMSD bond length	0.010
RMSD bond angle	0.052
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.500 *
Rmerge	0.061 *
Completeness [%]	95.3 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Batch method *	7.2 *	20 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	12 (mg/ml)
2	1	1	MOPS	50 (mM)
3	1	1	PEG8000	10-12 (%(w/v))