1PID
BOVINE DESPENTAPEPTIDE INSULIN
Experimental procedure
| Spacegroup name | C 1 21 1 |
| Unit cell lengths | 52.700, 26.180, 51.710 |
| Unit cell angles | 90.00, 93.00, 90.00 |
Refinement procedure
| Resolution | 25.400 - 1.300 |
| R-factor | 0.19 * |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.030 |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| Number of reflections | 31367 * |
| Completeness [%] | 90.7 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Batch method * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | depentapeptide insulin | 15 mg | |
| 2 | 1 | 1 | Tris-HCl | 0.02 (M) | 5.0ml |
| 3 | 1 | 1 | trisodium citrate | 0.05 (M) | 5.0ml |
| 4 | 1 | 1 | ammonium sulfate | 40 (%sat) | 1.5ml |
| 5 | 1 | 1 | acetone | 1.5ml | |
| 6 | 1 | 1 | citric acid | 0.1 (M) |
