1PE6
REFINED X-RAY STRUCTURE OF PAPAIN(DOT)E-64-C COMPLEX AT 2.1-ANGSTROMS RESOLUTION
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.900, 95.510, 49.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.100 |
R-factor | 0.159 |
RMSD bond length | 0.011 |
RMSD bond angle | 0.040 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.100 * |
Rmerge | 0.027 * |
Number of reflections | 12794 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 20 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | enzyme | 1.5 (%(w/v)) | |
2 | 1 | drop | 7.6 (mM) | ||
3 | 1 | drop | methanol | 42.6 (%(w/v)) | |
4 | 1 | drop | ethanol | 21.3 (%(w/v)) |