Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY |
| Synchrotron site | Photon Factory |
| Temperature [K] | 287 |
| Detector technology | WEISENBERG |
| Collection date | 1991-03-15 |
| Spacegroup name | I 41 3 2 |
| Unit cell lengths | 148.125, 148.125, 148.125 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 105.410 - 2.400 |
| R-factor | 0.194 |
| Rwork | 0.192 |
| R-free | 0.24200 |
| Structure solution method | MIR |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.491 |
| Data reduction software | WEIS |
| Data scaling software | SCALA |
| Phasing software | MLPHARE |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 100.000 |
| High resolution limit [Å] | 2.200 |
| Rmerge | 0.074 |
| Number of reflections | 12666 |
| Completeness [%] | 95.0 |
| Redundancy | 9.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | 2M NA/K PHOSPHATE PH 5.5 |
