1ODX

HIV-1 Proteinase mutant A71T, V82A

Experimental procedure

Temperature [K]	293
Detector technology	IMAGE PLATE
Collection date	1996-05-22
Detector	MARRESEARCH
Spacegroup name	P 61
Unit cell lengths	63.320, 63.320, 83.990
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 2.000
R-factor	0.166 *
Rwork	0.166
RMSD bond length	0.015
RMSD bond angle	0.047
Data reduction software	DENZO
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000
High resolution limit [Å]	2.000
Rmerge	0.084
Total number of observations	38546 *
Number of reflections	11019
Completeness [%]	85.2
Redundancy	3.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	sodium cacodylate	0.1 (M)
2	1	reservoir	sodium acetate	0.06 (M)
3	1	reservoir	PEG8000	25 (%)
4	1	reservoir	sodium azide	0.02 (%)