1NHX
PEPCK COMPLEX WITH A GTP-COMPETITIVE INHIBITOR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 1999-05-14 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 45.383, 61.452, 62.265 |
Unit cell angles | 89.71, 70.24, 72.56 |
Refinement procedure
Resolution | 50.000 - 2.100 |
R-factor | 0.17532 |
Rwork | 0.173 |
R-free | 0.21718 |
Structure solution method | RIGID-BODY REFINEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.131 |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.170 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 32199 | |
<I/σ(I)> | 23.5 | |
Completeness [%] | 91.3 | 84 |
Redundancy | 2.2 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * |