1NEL

FLUORIDE INHIBITION OF YEAST ENOLASE: CRYSTAL STRUCTURE OF THE ENOLASE-MG2+-F--PI COMPLEX AT 2.6-ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 42 21 2
Unit cell lengths	122.500, 122.500, 67.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 2.600
R-factor	0.169
RMSD bond length	0.013
RMSD bond angle	0.047
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.590 *	2.590 *
Rmerge	0.063 *
Total number of observations	63663 *
Number of reflections	17176 *
Completeness [%]		68 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	3 (%)
2	1	drop		2 (mM)
3	1	drop	EDTA	1 (mM)
4	1	drop	dithiothreitol	1 (mM)
5	1	drop	citrate	0.05 (M)
6	1	drop	ammonium sulfate	55 (%sat)
7	1	reservoir	ammonium sulphate	55 (%sat)