1NCO

STRUCTURE OF THE ANTITUMOR PROTEIN-CHROMOPHORE COMPLEX NEOCARZINOSTATIN

Experimental procedure

Spacegroup name	P 65
Unit cell lengths	90.400, 90.400, 52.500
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	? - 1.800
R-factor	0.199
RMSD bond length	0.014
RMSD bond angle	2.840
Phasing software	X-PLOR
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	1.700 *
Rmerge	0.071 *
Total number of observations	146707 *
Number of reflections	23556 *
Completeness [%]	87.8 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	5 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	20 (mg/ml)
2	1	drop	sodium acetate	50 (mM)
3	1	reservoir	MPD	70 (%)
4	1	reservoir	sodium acetate	50 (mM)