1N95
Aryl Tetrahydrophyridine Inhbitors of Farnesyltranferase: Glycine, Phenylalanine and Histidine Derivatives
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-04-04 |
Detector | MARRESEARCH |
Wavelength(s) | 1.000 |
Spacegroup name | P 61 |
Unit cell lengths | 171.126, 171.126, 69.404 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.590 - 2.300 |
Rwork | 0.337 |
R-free | 0.35800 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.014 |
RMSD bond angle | 1.800 * |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.590 | 2.400 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 43175 | |
Completeness [%] | 83.4 | 64 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * |