1MU8
thrombin-hirugen_l-378,650
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 290 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998 |
| Detector | RIGAKU RAXIS II |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 71.120, 72.230, 73.030 |
| Unit cell angles | 90.00, 100.80, 90.00 |
Refinement procedure
| Resolution | 25.000 - 2.000 |
| R-factor | 0.2088 |
| Rwork | 0.239 |
| Structure solution method | FOURIER SYNTHESIS |
| Data scaling software | SCALEPACK |
| Refinement software | CNX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 25.000 | 25.942 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 23202 | |
| Completeness [%] | 94.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 295 | pH 7.3, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
