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1MQI

Crystal Structure of the GluR2 Ligand Binding Core (S1S2J) in Complex with Fluoro-Willardiine at 1.35 Angstroms Resolution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X4A
Synchrotron siteNSLS
BeamlineX4A
Temperature [K]110
Detector technologyCCD
Collection date2000-04-06
DetectorADSC QUANTUM 4
Wavelength(s)0.9746
Spacegroup nameP 21 21 2
Unit cell lengths63.913, 91.431, 48.286
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.000

*

- 1.350
R-factor0.2
Rwork0.200
R-free0.21800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ftm
RMSD bond length0.005
RMSD bond angle1.220

*

Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareCNS (1.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.400
High resolution limit [Å]1.3501.350
Rmerge0.0460.190
Number of reflections57754
Completeness [%]91.1

*

52.1
Redundancy4.63
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.54

*

PEG 8K, NaCl, Na Citrate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein5 (mM)
21reservoirPEG800014-16 (%)
31reservoir0.2 (M)
41reservoirsodium citrate0.1 (M)pH5.5

222036

PDB entries from 2024-07-03

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