1LOA
THREE-DIMENSIONAL STRUCTURES OF COMPLEXES OF LATHYRUS OCHRUS ISOLECTIN I WITH GLUCOSE AND MANNOSE: FINE SPECIFICITY OF THE MONOSACCHARIDE-BINDING SITE
Experimental procedure
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 56.300, 139.800, 62.700 |
格子定数 [度] | 90.00, 91.00, 90.00 |
精密化法
残基 | 8.000 - 2.200 |
R因子 | 0.179 |
Rwork | 0.179 |
結合長の平均二乗偏差(RMSD) [Å] | 0.003 * |
結合角の平均二乗偏差(RMSD) [度] | 3.000 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Quality characteristics
Overall | |
分解能 [Å] (高) | 2.200 * |
Rmerge_l_obs | 0.082 * |
Total number of observations | 77034 * |
独立反射数 | 33640 * |
完全性 [%] | 67.0 * |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | Vapor diffusion, sitting drop * | 7.5 * | 20 * | reservoirs contain the same ingredients as drops, but twice as consentrated. taken from Bourne, Y. et al. (1988). J. Mol. Biol., 202, 685-687. * |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | MPD | 40 (%(v/v)) | |
3 | 1 | drop | 0.05 (M) | ||
4 | 1 | drop | HEPES | 0.02 (M) |