1LNL
Structure of deoxygenated hemocyanin from Rapana thomasiana
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 243 |
Detector technology | CCD |
Collection date | 2000-03-20 |
Detector | MARRESEARCH |
Wavelength(s) | 0.921 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 105.486, 105.486, 374.988 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 3.380 * |
R-factor | 0.24974 |
Rwork | 0.248 |
R-free | 0.28700 * |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.040 * |
RMSD bond angle | 3.100 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 3.383 |
High resolution limit [Å] | 3.380 * | 3.380 * |
Rmerge | 0.108 * | 0.373 * |
Total number of observations | 792618 * | |
Number of reflections | 33066 | |
Completeness [%] | 99.8 * | 99.7 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.8 * | 293 | Perbandt, M., (2001) Acta Crystallogr., D57, 1663. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 20 (mg/ml) | |
2 | 1 | reservoir | magnesium formate | 0.2 (M) | |
3 | 1 | reservoir | Tris-HCl | 20 (mM) | pH7.8 |