1LMW
LMW U-PA Structure complexed with EGRCMK (GLU-GLY-ARG Chloromethyl Ketone)
Experimental procedure
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Detector technology | IMAGE PLATE |
Collection date | 1994 |
Detector | FUJI |
Spacegroup name | H 3 |
Unit cell lengths | 176.700, 176.700, 54.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.500 |
R-factor | 0.224 |
Rwork | 0.224 |
RMSD bond length | 0.013 |
RMSD bond angle | 2.000 * |
Data reduction software | DENZO |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.111 |
Total number of observations | 54540 * |
Number of reflections | 15684 |
Completeness [%] | 70.0 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 13-14 (%) | |
2 | 1 | reservoir | 0.2 (M) |