1LFU
NMR Solution Structure of the Extended PBX Homeodomain Bound to DNA
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | DRX | 500 | |
| 2 | Varian | INOVA | 750 | |
| 3 | Varian | INOVA | 800 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 3D_15N-separated_NOESY |
| 2 | 1 | 1 | HNHA |
| 3 | 3 | 3 | 3D_13C-separated_NOESY |
| 4 | 4 | 4 | 2D NOESY |
| 5 | 5 | 5 | t1-1H coupled 15N HSQC |
| 6 | 6 | 6 | t1-1H coupled 13C HSQC, 13C HMQC |
| 7 | 1 | 1 | t1-1H coupled 15N HSQC |
| 8 | 4 | 4 | t1-1H coupled 13C HSQC, 13C HMQC |
| 9 | 3 | 3 | 13C filtered 2D NOESY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 7 | ambient | 303 |
| 2 | 7 | ambient | 303 |
| 3 | 7 | ambient | 303 |
| 4 | 7 | ambient | 303 |
| 5 | 6.6 | ambient | 310 |
| 6 | 6.6 | ambient | 310 |
Conformers
| Conformers Calculated Total Number | 100 |
| Conformers Submitted Total Number | 20 |
