1LAT
GLUCOCORTICOID RECEPTOR MUTANT/DNA COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 103 |
Detector technology | IMAGE PLATE |
Collection date | 1993-08-16 |
Detector | FUJI |
Wavelength(s) | 0.908 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.720, 76.070, 118.880 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.900 |
R-factor | 0.195 * |
Rwork | 0.195 |
R-free | 0.28100 |
RMSD bond length | 0.018 |
RMSD bond angle | 1.700 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 6.000 |
High resolution limit [Å] | 1.900 |
Rmerge | 0.060 |
Number of reflections | 26580 |
Completeness [%] | 96.6 |
Redundancy | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 4 * | pH 6.00, VAPOR DIFFUSION, HANGING DROP, temperature 277.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | ETHANOL | ||
3 | 1 | 1 | CACODYLATE | ||
4 | 1 | 1 | NACL | ||
5 | 1 | 1 | MG SULFATE | ||
6 | 1 | 1 | ZNCL2 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | E/TRGR-GRES0 complex | 0.1 (mM) | |
2 | 1 | drop | Na cacodylate | 0.02 (M) | |
3 | 1 | drop | 20 (mM) | ||
4 | 1 | drop | 8 (mM) | ||
5 | 1 | drop | 2 (mM) | ||
6 | 1 | reservoir | ethanol | 7 (%) | |
7 | 1 | reservoir | Na cacodylate | 36 (mM) | |
8 | 1 | reservoir | 200 (mM) |