1KTS
Thrombin Inhibitor Complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-09-11 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.54 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 69.900, 71.000, 72.200 |
| Unit cell angles | 90.00, 99.80, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.400 |
| R-factor | 0.211 |
| Rwork | 0.211 |
| R-free | 0.30900 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.009 * |
| RMSD bond angle | 1.890 * |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.400 |
| Rmerge | 0.063 |
| Total number of observations | 24556 * |
| Number of reflections | 11967 * |
| Completeness [%] | 89.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | Skrzypczak-Jankun, E., (1991) J. Mol. Biol., 221, 1379. * |
