1KQS
The Haloarcula marismortui 50S Complexed with a Pretranslocational Intermediate in Protein Synthesis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2000-09-29 |
Detector | CUSTOM-MADE |
Wavelength(s) | 1.033 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 212.784, 300.349, 574.961 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 3.100 |
R-factor | 0.1709 * |
Rwork | 0.173 |
R-free | 0.22050 * |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 1.333 |
RMSD bond angle | 2.161 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | 3.150 |
High resolution limit [Å] | 3.070 | 3.070 |
Total number of observations | 2581688 * | |
Number of reflections | 340617 * | |
Completeness [%] | 99.9 | 99.7 |
Redundancy | 7.6 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6 | 277 | data unknown * |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | PEG 6000 | ||
2 | 1 | 1 | KCl | ||
3 | 1 | 1 | NH4Cl | ||
4 | 1 | 1 | MgCl2 | ||
5 | 1 | 1 | CdCl2 | ||
6 | 1 | 1 | POTASSIUM ACETATE | ||
7 | 1 | 1 | TRIS-MES |