1JWT
CRYSTAL STRUCTURE OF THROMBIN IN COMPLEX WITH A NOVEL BICYCLIC LACTAM INHIBITOR
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 298 |
| Detector technology | IMAGE PLATE |
| Collection date | 1997-04-07 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 71.540, 72.180, 73.410 |
| Unit cell angles | 90.00, 100.99, 90.00 |
Refinement procedure
| Resolution | 25.000 - 2.500 |
| R-factor | 0.182 |
| Rwork | 0.182 |
| R-free | 0.30100 |
| Structure solution method | FOURIER SYNTHESIS |
| Data reduction software | AUTOMAR |
| Data scaling software | XDS |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 25.000 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 12595 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
