1INR
CYTOKINE SYNTHESIS
Experimental procedure
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, Hamburg |
Beamline | BW7B |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Collection date | 1994-09 |
Detector | MARRESEARCH |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 36.370, 36.370, 220.970 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
R-factor | 0.221 |
Rwork | 0.221 |
R-free | 0.33700 |
RMSD bond length | 0.020 |
RMSD bond angle | 21.840 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.080 |
Total number of observations | 42251 * |
Number of reflections | 10087 |
Completeness [%] | 92.0 * |
Redundancy | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.2 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium sulfate | 35 (%sat) | |
2 | 1 | 1 | HEPES | 100 (mM) |