1GSE
GLUTATHIONE TRANSFERASE A1-1 COMPLEXED WITH AN ETHACRYNIC ACID GLUTATHIONE CONJUGATE (MUTANT R15K)
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-01-20 |
Detector | RIGAKU RAXIS |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 100.400, 94.800, 51.800 |
Unit cell angles | 90.00, 92.96, 90.00 |
Refinement procedure
Resolution | 7.500 - 2.000 |
R-factor | 0.197 |
Rwork | 0.197 |
R-free | 0.24400 * |
RMSD bond length | 0.009 |
RMSD bond angle | 1.440 * |
Data reduction software | DENZO |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 15.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.073 |
Total number of observations | 64609 * |
Number of reflections | 30538 |
Completeness [%] | 93.4 |
Redundancy | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 20 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 55 (mg/ml) | |
2 | 1 | drop | PEG2000 | 10-20 (%) | |
3 | 1 | drop | Tris-HCl | 100 (mM) | |
4 | 1 | drop | NaAc | 30 (mM) | |
5 | 1 | drop | beta-mercaptoethanol | 1 (%) | |
6 | 1 | reservoir | PEG2000 | 10-20 (%) | |
7 | 1 | reservoir | Tris-HCl | 100 (mM) | |
8 | 1 | reservoir | NaAc | 30 (mM) | |
9 | 1 | reservoir | beta-mercaptoethanol | 1 (%) |