1GCW
CO form hemoglobin from mustelus griseus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-18B |
Synchrotron site | Photon Factory |
Beamline | BL-18B |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Detector | FUJI |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.700, 80.450, 114.830 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.000 |
R-factor | 0.199 |
Rwork | 0.199 |
R-free | 0.25500 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.090 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.075 | 0.265 |
Total number of observations | 260718 * | |
Number of reflections | 39951 * | |
Completeness [%] | 91.5 | 66.4 |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7 | 298 | PEG2000, sodium phosphate, hydro sulfide, pH 7.00, SMALL TUBES, temperature 298K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | PEG2000 | 8 (%(w/v)) | |
2 | 1 | 1 | sodium phosphate | 50 (mM) | |
3 | 1 | 1 | protein | 2 (%) |