1FKL
ATOMIC STRUCTURE OF FKBP12-RAPAYMYCIN, AN IMMUNOPHILIN-IMMUNOSUPPRESSANT COMPLEX
Experimental procedure
| Detector technology | IMAGE PLATE |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 48.900, 49.500, 55.200 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 7.000 - 1.700 |
| R-factor | 0.181 |
| Rwork | 0.181 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.240 * |
| Data reduction software | MANUFACTURER (SUPPLIED (MSC)) |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 5.5 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 10 (mg/ml) | |
| 2 | 1 | reservoir | ammonium sulfate | 50 (mM) | |
| 3 | 1 | reservoir | potassium phosphate | 200 (mM) |
