1FJL
HOMEODOMAIN FROM THE DROSOPHILA PAIRED PROTEIN BOUND TO A DNA OLIGONUCLEOTIDE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 72.210, 146.890, 77.230 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 * - 2.000 |
R-factor | 0.197 * |
Rwork | 0.198 |
R-free | 0.27000 * |
RMSD bond length | 0.018 |
RMSD bond angle | 2.800 |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 * | |
High resolution limit [Å] | 2.000 * | |
Rmerge | 0.058 * | 0.185 * |
Total number of observations | 94960 * | |
Number of reflections | 28315 * | |
Completeness [%] | 92.9 * | 83.3 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 5.5 * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | Na acetate | 100 (mM) | |
2 | 1 | 1 | 20 (mM) | ||
3 | 1 | 1 | PEG1000 | 19 (%(w/v)) | |
4 | 1 | 1 | ethylene glycol | 13 (%) | 2 % increments over 30 min. |