1FID

STRUCTURE OF HUMAN GAMMA FIBRINOGEN 30 KD CARBOXYL TERMINAL FRAGMENT

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1996-05-08
Detector	RIGAKU RAXIS II
Spacegroup name	P 21 21 2
Unit cell lengths	84.360, 62.560, 49.620
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.100
R-factor	0.17
Rwork	0.170
R-free	0.22600
RMSD bond length	0.009
RMSD bond angle	23.950 *
Data reduction software	DENZO
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000 *
High resolution limit [Å]	2.000 *
Rmerge	0.061
Number of reflections	16754
Completeness [%]	94.6
Redundancy	6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	6		pH 6.

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG8000	18 (%)
2	1	reservoir		70 (mM)
3	1	reservoir	MES	0.1 (M)