1FDJ
FRUCTOSE 1,6-BISPHOSPHATE ALDOLASE FROM RABBIT LIVER
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 293 |
Detector technology | AREA DETECTOR |
Collection date | 1994-11-10 |
Detector | XENTRONICS |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 377.250, 130.540, 80.030 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 12.000 - 2.100 |
R-factor | 0.174 |
Rwork | 0.171 |
R-free | 0.21400 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.770 |
Data reduction software | X-GEN |
Data scaling software | X-GEN |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 12.000 | 2.250 |
High resolution limit [Å] | 2.130 | 2.130 |
Rmerge | 0.092 | 0.180 |
Number of reflections | 85613 | |
<I/σ(I)> | 10.8 | |
Completeness [%] | 85.1 | 68.1 |
Redundancy | 4.5 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 277 | 45% saturated ammonium sulphate solution, 100mM Tris.HCl, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 277K |