1F9P

CRYSTAL STRUCTURE OF CONNECTIVE TISSUE ACTIVATING PEPTIDE-III(CTAP-III) COMPLEXED WITH POLYVINYLSULFONIC ACID

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	1999-09-01
Detector	RIGAKU RAXIS IV
Spacegroup name	P 43 21 2
Unit cell lengths	54.700, 54.700, 58.290
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.000 - 1.930
R-factor	0.232
Rwork	0.232
R-free	0.27200
RMSD bond length	0.008
RMSD bond angle	1.400
Data scaling software	SCALEPACK
Phasing software	EPMR
Refinement software	CNS (0.4)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.000
High resolution limit [Å]	1.930	1.930
Rmerge	0.063
Number of reflections	7080
<I/σ(I)>	47.8
Completeness [%]	99.6	97.5
Redundancy	15	10

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4	296	PEG 1000, sodium acetate, pH 4.0, VAPOR DIFFUSION, HANGING DROP, temperature 296K