1EXP
BETA-1,4-GLYCANASE CEX-CD
Experimental procedure
Detector technology | AREA DETECTOR |
Detector | XUONG-HAMLIN MULTIWIRE |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 88.172, 88.172, 81.097 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.800 |
R-factor | 0.208 |
Rwork | 0.208 |
R-free | 0.28300 |
RMSD bond length | 0.014 |
RMSD bond angle | 22.400 * |
Data reduction software | SDMS (DETECTOR SYSTEM (NIELSEN)) |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 8.000 * |
High resolution limit [Å] | 1.800 |
Rmerge | 0.041 |
Total number of observations | 139457 * |
Number of reflections | 29464 * |
Completeness [%] | 99.0 |
Redundancy | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4.6 * | Bedarkar, S., (1992) J.Mol. Biol, 228, 693. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | Cex | 65 (mg/ml) | in water |
2 | 1 | drop | PEG4000 | 7.5-10 (%) | |
3 | 1 | drop | sodium acetate | 0.1 (M) | |
4 | 1 | reservoir | PEG4000 | 7.5-10 (%) | |
5 | 1 | reservoir | sodium acetate | 0.1 (M) |