1EQP
EXO-B-(1,3)-GLUCANASE FROM CANDIDA ALBICANS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1993-05-12 |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 60.100, 65.300, 96.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.900 |
R-factor | 0.154 |
Rwork | 0.156 |
R-free | 0.19500 |
RMSD bond length | 0.013 |
RMSD bond angle | 0.025 |
Data reduction software | ROTAVATA |
Data scaling software | CCP4 ((AGROVATA) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.000 | 2.010 |
High resolution limit [Å] | 1.900 * | 1.900 |
Rmerge | 0.035 | 0.103 |
Number of reflections | 26304 | |
<I/σ(I)> | 14.2 | |
Completeness [%] | 90.3 | 56.6 * |
Redundancy | 2.5 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 291 | Chambers, R.S., (1993) J. Gen. Microbiol., 139, 325., Chambers, R.S., (1993) FEBS Lett., 327, 366. * |